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- W2029041687 abstract "Reaction of [ M ~ O C l ~ ( t h f ) ~ ] with aromatic thiols HSAr (Ar = Ph or 4-MeC6H4) and sodium methoxide/methanol yields the complex ions [ M O ~ O ~ ( S A ~ ) ~ ( O M ~ ) ] , which have been obtained as crystalline [Et,N]+ salts. The structure of [ Et,N] [ M O ~ ~ ~ ( ~ M ~ C ~ H ~ S ) ~ ( O M ~ ) ] has been determined by single-crystal X-ray diffraction. Crystals are orthorhombic, space group P21212, with a = 26.416 (4) A, b = 41.380 (6) A, c = 15.237 (2) A, and Z = 12. Refinement, based on 7034 diffractometer data, gave R = 0.1 10. There are three crystallographically independent anions, each with two terminal oxo groups, four terminal and two bridging thiolate ligands, and a bridging methoxy ligand, arranged around a Moz center with Mo-Mo = 2.919 ( 5 ) A." @default.
- W2029041687 created "2016-06-24" @default.
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- W2029041687 date "1984-02-21" @default.
- W2029041687 modified "2023-09-24" @default.
- W2029041687 title "ChemInform Abstract: TRIPLY BRIDGED BINUCLEAR COMPLEXES OF OXOMOLYBDENUM(V) WITH THIOLATE LIGANDS" @default.
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- W2029041687 doi "https://doi.org/10.1002/chin.198408249" @default.
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