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• W2029166411 startingPage "837" @default.
• W2029166411 abstract "Abstract A new pulse sequence, 2D INEPT‐PANACEA, that allows parallel acquisition of 2D 29 Si 29 Si INADEQUATE and 2D 29 Si 1 H HMBC spectra and also provides the 1D 29 Si NMR spectrum has been designed for use with organosilicon compounds and tested using a mixture of OH‐terminated polydimethylsiloxanes. The spectra provide 29 SiO 29 Si connectivities and multiple bond 29 Si 1 H correlation spectra in a single measurement that can be recorded in as little time as 8 min. In addition, the 1D 29 Si NMR spectrum provides accurate measurement of 29 Si chemical shifts with a signal‐to‐noise ratio allowing for determination of 29 Si 13 C spin–spin coupling constants, and also serves as a frequency lock. The latter feature allows for recording of NMR spectra of neat liquid samples or of samples without a deuterated solvent. The second example of using multiple receivers involves PANSY‐COSY and PANSY‐TOCSY experiments, using silatrane glycol as a test sample. Copyright © 2010 John Wiley & Sons, Ltd." @default.
• W2029166411 created "2016-06-24" @default.
• W2029166411 creator A5062402824 @default.
• W2029166411 creator A5079183378 @default.
• W2029166411 date "2010-11-23" @default.
• W2029166411 modified "2023-10-16" @default.
• W2029166411 title "Multiple receiver experiments for NMR spectroscopy of organosilicon compounds" @default.
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• W2029166411 doi "https://doi.org/10.1002/aoc.1692" @default.
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