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- W2029182495 abstract "A RECENT report1,2 describes the effect on Raney platinum electrodes of cathodic pretreatment in 10N H2SO4. Current-voltage curves for the oxidation of formic acid in 3N H2SO4 before and after pretreatment were compared and the enhanced currents measured for the treated electrodes were attributed to an adsorbed layer of sulphur formed by deposition during the cathodic pretreatment. This is surprising because the inhibiting effect of sulphur adsorbed on platinum on many other surface reactions and electrode reactions is well known and was observed by Faraday3. Enhanced catalytic activity was also observed1,2 by using electrodes pretreated with gaseous hydrogen sulphide at high temperatures and with electrodes cathodically polarized in solutions of selenium oxide in dilute sulphuric acid. Extended cathodic pretreatment in 10 N H2SO4 yielded a less active electrode. Here, the sulphur was said to have formed a monolayer." @default.
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- W2029182495 date "1968-03-01" @default.
- W2029182495 modified "2023-09-24" @default.
- W2029182495 title "Enhanced Catalytic Activity of Platinum Electrodes resulting from Cathode Pretreatment" @default.
- W2029182495 cites W1990342869 @default.
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- W2029182495 doi "https://doi.org/10.1038/2171047a0" @default.
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