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• W2029210992 abstract "Abstract The reaction of meso-tetraarylporphyrins (H2t(Xp)p) with SbCl3 under free solvent conditions affords green complexes with a 1:1 H2t(X)pp:SbCl3 ratio. These complexes have dimeric structures with a (μ-Cl)2bridge. UV–VIS, 1H NMR and 13C NMR spectra data show that the porphyrin core of [(H2t(Xp)p)2Sb2Cl6], similar to 1:2 (donor:acceptor) molecular complexes of meso-tetraarylporphyrins and porphyrin diacid, is distorted, thus two nitrogen atoms of pyrrolenine in a side of the porphyrin plane act as electron donors to an antimony atom of SbCl3. Molecular complexation of meso-tetraarylporphyrins with SbCl3 produces a large downfield shift for the NH signal, although there is no hydrogen bonding present." @default.
• W2029210992 created "2016-06-24" @default.
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• W2029210992 date "2007-09-01" @default.
• W2029210992 modified "2023-09-25" @default.
• W2029210992 title "Molecular complexation of free base meso-tetraarylporphyrins with antimony(III) chloride in free solvent media" @default.
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• W2029210992 doi "https://doi.org/10.1016/j.poly.2007.05.044" @default.
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