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- W2029220132 abstract "The crystallization of CuCl-assisted dimerization of 2-bromo-3,4-bis(diphenylmethylene)cyclobutanone revealed two polymorphs (3 and 4). The dimer was intended to be a precursor to bis-radialenes. Attempts to dehydrogenate the compound to the true bis-radialene failed. This failure may be attributed to the overcrowding of the precursor. Dimerization was not observed in a similar reaction of 2,2-dibromo-3,4-bis(diphenylmethylene)cyclobutanone, and 5 was the only product obtained. The crystal structures of the three products are described. The overcrowding expressed by torsion angles is calculated, and experimental conformations of the central ring are compared for [3], [4], [5], and [6]radialenes." @default.
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- W2029220132 date "1999-03-12" @default.
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- W2029220132 title "Effect of Overcrowding in [<i>n</i>]Radialenes on the Synthesis of Bis[4]radialenes" @default.
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- W2029220132 doi "https://doi.org/10.1021/jo9818677" @default.
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