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- W2029233432 endingPage "175702" @default.
- W2029233432 startingPage "175702" @default.
- W2029233432 abstract "This study attempts to survey the influence of microwave irradiation on the characterizations of titanate nanotubes (TNTs) synthesized by microwave hydrothermal treatment (M-H treatment). Based on the performance of specific surface areas determined by the classic Brunauer–Emmett–Teller method (SBET), TNTs synthesized at 130 °C for 1.5 h with and without 400 W irradiation presented SBET values of 256 and 76 m2 g−1, respectively. The result indicates that the formation kinetics of TNTs is significantly enhanced by M-H treatment. The microwave-induced TNTs are preferentially assigned for NaxH2−xTi3O7 structure and the Na/H ratio appreciably increases with higher irradiation power. Regarding the behaviour of TNTs after thermal treatment, TNTs synthesized under 70 W presented anatase phase at 500 °C through rearrangement and restacking of [TiO6 ]. Anatase-to-rutile transformation subsequently occurred at 700 °C. TNTs synthesized under 400 and 700 W presented a rod shape at 700 °C. The rod shape mainly comprise of Na2Ti6O13 of which the (Ti3O7)2− layers with the topotactical connection proceed to form (Ti6O13)2− along the [110] direction during the thermal process." @default.
- W2029233432 created "2016-06-24" @default.
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- W2029233432 date "2007-04-02" @default.
- W2029233432 modified "2023-10-17" @default.
- W2029233432 title "Microwave-induced titanate nanotubes and the corresponding behaviour after thermal treatment" @default.
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- W2029233432 doi "https://doi.org/10.1088/0957-4484/18/17/175702" @default.
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