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• W2029451011 abstract "The electrochemical preparation of europium doped zinc oxide and europium oxide/hydroxide as thin films is investigated. First, a thermodynamic study of the Eu–Cl–H2O system has been carried out at 25 and 70 °C in order to predict the electrochemical behaviour of Eu(III) dissolved in aqueous solution containing chloride ions. A comparison of the Eu–Cl–H2O and Zn–Cl–H2O systems indicates the possible coprecipitation of ZnO and Eu(OH)3 from deposition solutions containing well-adjusted Eu(III)/Zn(II) concentrations ratio. The thermodynamic predictions have been confirmed experimentally by the electrochemical co-deposition of ZnO/Eu thin films on conducting electrode substrates at −1.4 V versus MSE. The presence of europium in the film is detected for Eu(III)/Zn(II) concentration ratio at (0.6 mM/5 mM) which is lower than the predicted value. Increasing Eu(III) concentration leads to the rapid appearance of two phases: dispersed zinc oxide nanorods and, at the bottom of the rods, a covering layer containing Eu(OH)3 and zinc. The density of ZnO rods decreases and the rod size increases with increasing Eu(III) concentration in the bath. Above 1 mM EuCl3, a dramatic fall in the current density is observed with the formation of a less conducting ZnO/Eu mixed deposit." @default.
• W2029451011 created "2016-06-24" @default.
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• W2029451011 date "2007-11-01" @default.
• W2029451011 modified "2023-10-14" @default.
• W2029451011 title "Preparation of ZnO/Eu mixed films by electrochemical precipitation" @default.
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• W2029451011 doi "https://doi.org/10.1016/j.electacta.2007.01.036" @default.
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