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• W2029509301 endingPage "2727" @default.
• W2029509301 startingPage "2723" @default.
• W2029509301 abstract "The complex [NEt4]2[Fe2S2(tmbt)4](tmbt = 2,4,6-trimethylbenzenethiolate) was synthesised and its molecular structure determined. The crystal system is monoclinic with a= 15.241(6), b= 16.174(5), c= 16.768(6)Å, β= 135.84(2) and Z= 2, in space group P21/c. The Fe–S*(S*= inorganic sulphide) bond lengths are 2.195(6) and 2.204(6)Å and the Fe–S(C) are 2.299(8) and 2.318(6)Å. Steric congestion at the thiolate ligands causes rotation of two of the for Fe–S(C) torison angles from the stable staggered position to the restrictedly eclipsed position. The eclipsed Fe–S(C) has a wide Fe–S–C angle [112.35(76)°] with π-bond character and another staggered Fe–S(C) possesses a narrow Fe–S–C angle [104.95(64)°] with less π-bond character." @default.
• W2029509301 created "2016-06-24" @default.
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• W2029509301 date "1991-01-01" @default.
• W2029509301 modified "2023-10-16" @default.
• W2029509301 title "Synthesis, crystal structure and electronic properties of a 2Fe–2S complex with a bulky thiolato ligand, [NEt₄]₂[Fe₂S₂(SC₆H₂Me₃-2,4,6)₄]" @default.
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• W2029509301 doi "https://doi.org/10.1039/dt9910002723" @default.
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