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- W2029587572 abstract "Abstract Utilizing polymer-bound anthranilic acid derivatives, we were able to obtain 3,4-dihydro-1H-2,1-benzothiazine-4-one 2,2-dioxide derivatives through N-methanesulfonylation by use of sulfonyl chloride, sulfonic acid, or sodium sulfonate, N-alkylation under Mitsunobu condition, and the cyclative cleavage in 8–52% five-step overall isolated yields and 91–99% purities from Wang resin. The reactions on solid phase were monitored by on-bead ATR-FTIR spectroscopic method and checked by help of solution-phase model experiments." @default.
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- W2029587572 date "2008-09-01" @default.
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- W2029587572 title "A solid-phase synthetic method for 3,4-dihydro-1H-2,1-benzothiazin-4-one 2,2-dioxide derivatives" @default.
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- W2029587572 doi "https://doi.org/10.1016/j.tet.2008.07.031" @default.
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