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- W2029971337 abstract "The mechanisms of the first two stages of the thermal decomposition of calcium oxalate monohydrate have been established from non-isothermal thermogravimetric studies. For both stages, the rate-controlling processes are phase boundary reactions; the dehydration step assumes spherical symmetry whereas the decomposition step follows cylindrical symmetry. The kinetic parameters calculated from mechanistic equations show the same trend as those from mechanism-non-invoking equations. Thus, for the decomposition of CaC2O4 the kinetic parameters are not appreciably affected by heating rate or sample mass. For the dehydration step they show a systematic decrease with increase in either heating rate or sample mass. The best fit correlations can be expressed as follows E(or, log A) = (Constant/Heating rate) + Constant, (at fixed sample mass) E(or, log A) = (Constant) × (Mass)2 − (Constant) × (Mass) + Constant, (at fixed heating rate)" @default.
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- W2029971337 date "1979-05-01" @default.
- W2029971337 modified "2023-09-23" @default.
- W2029971337 title "Thermal decomposition kinetics. Part XI. Mechanism of thermal decomposition of calcium oxalate monohydrate from a thermogravimetric study — the effects of heating rate and sample mass on kinetic parameters from mechanistic equations" @default.
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- W2029971337 doi "https://doi.org/10.1016/0040-6031(79)85038-8" @default.
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