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- W2030131408 abstract "AbstractThe synthesis of α-aminooxy trisaccharide moiety [α-d-Gal-(1,4)-β-d-Gal-(1,4)-β-d-Glc-α-aminooxy], related to the cell surface globotriaosylceramide (Gb3) receptor of the B subunit of the AB5 Shiga toxin of Shigella dysenteriae, has been carried out for the first time in 11 steps with a 15% overall isolated yield. A highlight of this work entails utilizing chemically compatible synthetic transformations, including those related to glycosylation, incorporative of the succinimidyl moiety as a precursor to the aminooxy Gb3 derivative. The fully deprotected trisaccharide aminooxy compound was reacted with a carbonyl compound, leading to oxime formation in quantitative yield, which underscores the importance for future glyco-conjugations.Keywords: Aminooxy sugarGb3 trisaccharideShiga toxinGlycosylation" @default.
- W2030131408 created "2016-06-24" @default.
- W2030131408 creator A5065244217 @default.
- W2030131408 creator A5076217513 @default.
- W2030131408 date "2014-06-23" @default.
- W2030131408 modified "2023-10-07" @default.
- W2030131408 title "Synthesis of an Aminooxy Derivative of the Trisaccharide Globotriose Gb3" @default.
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- W2030131408 doi "https://doi.org/10.1080/07328303.2014.925913" @default.
- W2030131408 hasPubMedCentralId "https://www.ncbi.nlm.nih.gov/pmc/articles/4219983" @default.
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