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• W2030222018 abstract "The chiral intermediate diol (3S,4R)-trans-3,4-dihydro-3,4-dihydroxy-2,2-dimethyl-2H-1-benzopyran-6-carbonitrile2. was prepared for the total synthesis of a potassium channel opener drug candidate. The stereoselective acetylation of racemic 1 was carried out with various lipases among which the lipases from Candida cylindraceae and Pseudomonas cepacia catalyzed the acetylation of the undesired enantiomer of racemic 1 to yield monoacetylated product and unreacted desired (+)-trans diol 2. A reaction yield of >40% and an optical purity >90% were obtained using each lipase." @default.
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• W2030222018 date "1995-01-01" @default.
• W2030222018 modified "2023-09-27" @default.
• W2030222018 title "Stereoselective acetylation of 3,4-dihydro-3,4-dihydroxy-2,2-dimethyl-2H-1-benzopyran-6-carbonitrile" @default.
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• W2030222018 doi "https://doi.org/10.1016/0957-4166(94)00367-k" @default.
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