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- W2030343453 abstract "Abstract The synthesis of (Z)-2-methyl-3-triphenylstannyl-3-pentene-2-ol and its characterization by an X-ray diffraction study and multinuclear NMR are reported. The tin atom exhibits a distorted tetrahedral SnC 4 geometry with the four SnC bond distances experimentally equivalent. The slight distortion from the ideal tetrahedral geometry is because of the presence of a weak intramolecular HO → Sn interaction of 3.012(3) A which produces a loose four-membered ring. The title compound was characterized in solution by 1 H, 13 C and 119 Sn NMR, and the persistence of the weak intramolecular HO → Sn coordination in solution was revealed by 13 C and 119 Sn secondary isotope multiplet of partially labelled entities (SIMPLE-NMR) experiments." @default.
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- W2030343453 date "1994-10-01" @default.
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- W2030343453 title "Synthesis, X-ray diffraction analysis and NMR studies of (Z)-2-methyl-3-triphenylstannyl-3-pentene-2-ol" @default.
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- W2030343453 doi "https://doi.org/10.1016/0022-328x(94)87126-4" @default.
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