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- W2030377266 abstract "The mechanistic aspects of the one-pot C-acylation of cyclic 1,3-diones are discussed. Using various substituted carboxylic acids, coupling agents and basic catalysts we aim to describe the process of direct transfer of an acyl group to the activated C-2 carbon of dimedone and 1,3-cyclohexanedione. The course of acylation was studied by high-performance liquid chromatography as well as on-line infrared spectroscopy. The results indicate that the direct acylation follows a nucleophilic acyl substitution mechanism rather than a nucleophilic attack on a ketene intermediate formed in situ from the activated carboxylic acid." @default.
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- W2030377266 date "2015-05-01" @default.
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- W2030377266 title "Mechanistic aspects of the direct C-acylation of cyclic 1,3-diones with various unactivated carboxylic acids" @default.
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- W2030377266 doi "https://doi.org/10.1016/j.tet.2015.03.037" @default.
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