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- W2030588809 abstract "ESR spectra are observed for the anion radicals of methyl p-, m- and o-nitrobenzoates, methyl ester of p-phthalaldehydic acid, and methyl and ethyl p-cyanobenzoates. Both the electrolytic and alkali-metal reduction methods are used for the radical generation. The spin densities calculated by McLachlan’s procedure only with the adjustment of the resonance-integral parameter for the ester group-ring bond are in good agreement with those obtained experimentally for most of the substituted positions in these radicals. The result for the methyl o-nitrobenzoate anion suggests that the ester group is twisted considerably by the large steric hindrance between the ester and nitro groups. The ring-proton splittings of three p-substituted methyl benzoate anions show that the known order of electron-withdrawing effects of the substituents, NO2>CHO>COCH3>COOCH3>CN, holds also for these anions. And it is suggested that the electron-withdrawing power of a XM+ group produced on the alkali-metal reduction increases in the..." @default.
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- W2030588809 date "1968-07-01" @default.
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- W2030588809 title "Electron Spin Resonance of Anion Radicals of Aromatic Esters. IV. The Anion Radicals of Some Substituted Methyl Benzoates" @default.
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- W2030588809 doi "https://doi.org/10.1246/bcsj.41.1502" @default.
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