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• W2030629203 abstract "The single crystals of the superconducting Li0.2(1)ZrNCl have been derived from the single crystals of β-ZrNCl by intercalation of lithium using an n-butyllithium solution in hexane. The crystal structure has been refined on the basis of the single-crystal X-ray data: the space group R-3m, a=3.591(1) Å, c=27.839(6) Å, Z=6, R1=0.0749 for 196 reflections and 12 variables. β-ZrNCl is isotypic with SmSI, while the structure of Li0.2(1)ZrNCl can be described as the Li intercalated YOF type, a stacking variant of the SmSI type. The tightly bound slabs with a Cl–Zr–N–N–Zr–Cl sequence of close-packed layers are stacked rhombohedrally along the c-axis, with the van der Waals gaps between the chlorine layers hosting Li ions. This is the first single-crystal study on the Li intercalated phase. The structural changes from the pristine single crystals were precisely determined." @default.
• W2030629203 created "2016-06-24" @default.
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• W2030629203 date "2002-12-01" @default.
• W2030629203 modified "2023-09-26" @default.
• W2030629203 title "The first single-crystal X-ray structural refinement of the superconducting phase Li0.2(1) ZrNCl derived by intercalation" @default.
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• W2030629203 doi "https://doi.org/10.1016/s0022-4596(02)00034-8" @default.
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