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• W2030716475 abstract "Nine different substituted cyclopentadienyl ligands, which have substituents that may either chelate or bridge to second metal center, have been prepared from nucleophilic substitution reactions of esters or alkyl halides with NaCp. The sodium or thallium salts of these ligands were isolated as solids and characterized by 1H NMR. The alkyl halide and NaCp reaction proved to yield the purer salts of the ligands because of the milder reaction conditions. These salts were reacted futher with Mn(CO)5Br to form the corresponding manganese tricarbonyl derivatives (i.e. (C5H4R)Mn(CO)3; where R = C(O)CH2OCH3, C(O)CH2SCH3, C(O)CH2CH2SCH3, CH2CO2CH3, CH2CO2CH2CH3, CH2CH2CO2CH3, CH2CH2CO2CH2CH3, CH2CH2O2CCH3, and CH2CH2OCH3) and Na(C5H4C(O)CH2OCH3) was reacted with Co2(CO)8 to form (C5H4C(O)CH2OCH3)Co(CO)2. The manganese and cobalt compounds were characterized by elemental analysis, IR, 1H, and 13C NMR spectra." @default.
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• W2030716475 date "1996-03-01" @default.
• W2030716475 modified "2023-09-26" @default.
• W2030716475 title "Synthesis and characterization of substituted cyclopentadienide ligands that may form chelates or metal dimers" @default.
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• W2030716475 doi "https://doi.org/10.1016/0022-328x(95)05802-v" @default.
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