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- W2030905036 abstract "The formation of protective or non-protective oxide scales on γ-TiAl alloys is closely related to the composition of the subsurface depletion layer. Recently it was shown that in the depletion layer a cubic Z-phase is formed, which was until then not known in the TiAlO phase diagram. In the present study a method was developed to synthesise this cubic phase by a powder metallurgical method. It was found that the Z-phase can be produced by a reaction between the α-TiOx solid solution and aluminium using self-propagating high temperature synthesis (SHS). The phase analysis and microstructural characterisation of the Ti-O-Al sintering products show that at 900–950 °C the Z-phase exists in equilibrium with γ-TiAl(O) and α-Al2O3, as well as with Ti2O and α2-Ti3Al(O) ordered solid solutions. According to X-ray and electron diffraction data the Z-phase has a primitive cubic structure of one of the space groups P 213 or P 4132 and has a composition close to Ti5Al3O2. The lattice parameter of the cubic phase was determined to be a = 0.691 ± 0.001 nm." @default.
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- W2030905036 date "1997-01-01" @default.
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- W2030905036 title "Synthesis of the cubic Z-phase in the TiAlO system by a powder metallurgical method" @default.
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- W2030905036 doi "https://doi.org/10.1016/s0966-9795(96)00091-x" @default.
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