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- W2030920453 abstract "Polymer microspheres with poly(methacrylic acid) (PMMA) core and poly(styrene) shell were synthesized from poly(styrene-b-methacrylic acid) (SAI, Mn = 5.35 × 104, methacrylic acid = 19.7 mol%) by casting from dioxane with hexamethylenediamine and N,N′-dicyclohexyl carbodiimide as the crosslinking reagents. The optimum amounts of the crosslinking reagents (C = [NH2]/[COOH]) were between 20 and 40 mol%. From the results of transmission electron microscopy and turbidimetric titration, the microsphere SA1-20M prepared with C = 20 mol% had a soft PMAA core and was flattened on the carbon substrate. The PMAA core of microsphere SA1-40M with C = 40 mol% was hard. From turbidimetric titration in the THF/water system, it was found that the soft microsphere SA1-20M was more swollen than SA1-40M." @default.
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- W2030920453 date "1991-01-01" @default.
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- W2030920453 title "Core-shell type polymer microspheres prepared from poly(styrene-b-methacrylic acid)—1. Synthesis of microgel" @default.
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- W2030920453 doi "https://doi.org/10.1016/0014-3057(91)90093-4" @default.
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