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- W2031014750 abstract "The thermal behavior of graphite oxide (GO) is essential to study and design GO reduction and functionalizion reaction. We provide a detailed description of the thermal reduction of GO dispersed in solvent (H2O and dimethylformamide (DMF)) at temperatures of 100 and 150 °C, respectively. The thermal stability and structure change of GO during the thermal treatment were characterized using UV−vis spectroscopy, Raman spectroscopy, X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FTIR), X-ray photoelectron spectroscopy (XPS), and thermogravimetric analysis (TGA). It was found that at temperatures of 100 and 150 °C the carboxylic and carbonyl groups decomposed. GO dispersed in H2O and DMF at temperatures of 100 and 150 °C exhibited increased rates of reduction than in dry condition. Moreover, the reduction rate was found to be highly dependent on the solvent used. At 150 °C, DMF accelerates the GO reduction rate significantly, while dimethyl sulfoxide (DMSO) has less acceleration effect. However, ethylene glycol (EG) reduces the reduction rate compared to dry conditions. The solvent−GO interaction, including polar−polar interaction and hydrogen bonding, was discussed as one possible reason for the solvent-dependent reduction." @default.
- W2031014750 created "2016-06-24" @default.
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- W2031014750 date "2010-08-19" @default.
- W2031014750 modified "2023-09-25" @default.
- W2031014750 title "Solvent-Assisted Thermal Reduction of Graphite Oxide" @default.
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- W2031014750 doi "https://doi.org/10.1021/jp1049843" @default.
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