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- W2031188788 abstract "A gradient elution method with conventional electrochemical detection was developed to separate four analogs of the nitroxide 2,2,6,6-tetramethyl-1-piperidinyloxy (TEMPO) free radical in less than 3 min. The corresponding hydroxylamines and oxoammonium ions of these free radicals were separated using the identical chromatographic method. A dual microelectrochemical detector was constructed that allowed for simultaneous anodic and cathodic detection of all three redox forms. This detector was superior to a conventional electrochemical detector because it could provide immediate information about the oxidation state of the nitroxide, it nearly eliminated post-column band broadening, and it was less susceptible to changes in oxygen concentration of the mobile phase during gradient elutions." @default.
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- W2031188788 date "1997-05-01" @default.
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- W2031188788 title "Separation of cyclic nitroxide free radicals and their redox forms with dual microelectrochemical detection" @default.
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