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• W2031239186 abstract "The structurally chiral [7-(2'-pyridyl)-7,8-nido-C(2)B(9)H(11)](-), [](-), anion was prepared by a partial degradation reaction of 1-(2'-pyridyl)-1,2-closo-C(2)B(10)H(11). From this anion a protonated specie, H[7-(2'-pyridyl)-7,8-nido-C(2)B(9)H(11)] , and a tetramethylammonium salt, [NMe(4)][7-(2'-pyridyl)-7,8-nido-C(2)B(9)H(11)], [NMe(4)][] can be obtained. The (1)H{(11)B} DNMR study on in the temperature range from 298 to 203 K identified the weakly basic nitrogen atom in the pyridine ring as the proton accepting site in solid state and low temperature and revealed pronounced weakening of the nitrogen-proton interaction while the temperature increases. Capillary electrophoresis and X-ray diffraction confirmed the pyridine nitrogen atom as the proton binding site. Separation of the electrophoretically pure racemic [7-(2'-pyridyl)-7,8-nido-C(2)B(9)H(11)](-) ion into two peaks by the chiral selector beta-cyclodextrine has been achieved." @default.
• W2031239186 created "2016-06-24" @default.
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• W2031239186 date "2007-01-01" @default.
• W2031239186 modified "2023-10-16" @default.
• W2031239186 title "Synthesis and investigation of the boron cluster anion [7-(2′-pyridyl)-7,8-nido-dicarbaundecaborate] and its protonated form" @default.
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• W2031239186 doi "https://doi.org/10.1039/b705160c" @default.
• W2031239186 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/17664973" @default.
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