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- W2031415905 abstract "A series of well-ordered mesoporous ZrO2-based heteropoly acid nanocomposite frameworks has been prepared through a surfactant-assisted sol–gel copolymerization route. The pore walls of these materials consist of nanocrystalline tetragonal ZrO2 and Keggin-type 12-phosphomolybdic acid (PMA) components with different PMA loadings, i.e. 12, 22 and 37 wt%. Small angle X-ray scattering, high-resolution TEM and N2 physisorption measurements indicated mesoporous property in hexagonal p6mm symmetry with large internal BET surface areas and narrow-sized pores. The incorporated PMA clusters preserve intact their Keggin structure into the mesoporous frameworks according to EDX, FT-IR and diffuse-reflectance UV/vis/NIR spectroscopy. The obtained ZrO2–PMA nanocomposites demonstrated great application potential in oxidative catalysis, exhibiting exceptional stability and catalytic activity in oxidation of alkenes using hydrogen peroxide as oxidant." @default.
- W2031415905 created "2016-06-24" @default.
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- W2031415905 date "2011-01-01" @default.
- W2031415905 modified "2023-10-14" @default.
- W2031415905 title "Highly ordered mesoporous zirconia-polyoxometalate nanocomposite materials for catalytic oxidation of alkenes" @default.
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- W2031415905 doi "https://doi.org/10.1039/c0jm03395b" @default.
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