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- W2031484585 abstract "The reaction between Ru3(CO)12 and a cyclic olefin (cis-cyclooctene or trans-cyclododecene) at 100 °C for several hours gives the title compounds (μ-H)2RU3(CO)9(μ3-η2-C8H12) (1), and (μ-H)RU3(CO)9(μ3-η3-C12H19) (2), both of which have been characterized by X-ray diffraction studies, IR and NMR spectral measurements and elemental analysis. The prolonged reaction between Ru3(CO)12 and cis-cyclooctene gives compound HRu3(CO)9(C8H11) (3). Compound 3 has been characterized with IR and NMR spectral analyses. In 1 the cyclooctene ring is linked via a μ3-η2-alkyne type of bonding to the face of the Ru3 cluster. It is formally σ-bonded to two of the three Ru atoms and π-bonded to the third Ru. The two hydrides in 1 are bridging RuRu bonds. In 2 the cyclododecene ring is bonded to the Ru3 face via the μ3-η3-CCHC linkage. There are two formal σ-bonds from the allyl part to the hydrido-bridged Ru atoms and the η3-allyl linkage to the third Ru atom." @default.
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- W2031484585 date "1996-03-01" @default.
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- W2031484585 title "Synthesis and structural characterization of (μ-H)2RU3(CO)9(μ3-η2-C8H12) and (μ-H)RU3(CO)9(μ3-η3-C12H19)" @default.
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- W2031484585 doi "https://doi.org/10.1016/0022-328x(95)05831-9" @default.
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