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• W2031489293 endingPage "1590" @default.
• W2031489293 startingPage "1585" @default.
• W2031489293 abstract "Crystal structure of an oxo-benzoate-bridged trinuclear ruthenium complex, [Ru3(μ3-O)(μ-C6H5COO)6(py)3](PF6) (py = pyridine) (1), was determined for the first time for the complexes with a Ru3(III,III,III)(μ3-O) core. The complex crystallizes in hexagonal space group P63 with a = 13.619(6), c = 19.204(9) A, V = 3085(3) A3, and Z = 2. The Ru···Ru distance of 3.350(2) A is similar to those of the trinuclear complexes of other metal ions, [MIII3(μ3-O)(μ-RCOO)6(L)3]+ (L = neutral unidentate ligand). The complex in 0.1 M (n-C4H9)4NPF6-acetonitrile at 20 °C shows four reversible one-electron processes at E1⁄2 = +1.58, +0.71, −0.26, and −1.54 V vs. Ag/Ag+ (0.1 M AgClO4). It undergoes pyridine-d5 exchange with the first-order rate constant, 4.9 × 10−6 s−1 at 60 °C ([1] = 4.7 mM, [py-d5] = 387 mM). Small modification of the synthetic procedure of the trinuclear complex leads to the precipitation of the crystals of well-known type of dimeric ruthenium (II,III) complex, [Ru2(μ-C6H5COO)4Cl], which crystallizes in mon..." @default.
• W2031489293 created "2016-06-24" @default.
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• W2031489293 date "1992-06-01" @default.
• W2031489293 modified "2023-10-06" @default.
• W2031489293 title "X-Ray Structure, Ligand Substitution, and Other Properties of Trinuclear Ruthenium Complex, [Ru₃(μ₃-O)(μ-C₆H₅COO)₆(py)₃](PF₆) (py = pyridine), and X-Ray Structure of Dinuclear Ruthenium Complex, [Ru₂(μ-C₆H₅COO)₄Cl]" @default.
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• W2031489293 doi "https://doi.org/10.1246/bcsj.65.1585" @default.
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