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- W2031490147 abstract "Highly selective techniques of gas chromatography mass spectrometry have been used in the unequivocal identification of salivary steroids at concentrations ranging from 20 pg ml−1 to 20 ng ml−1. Oestradiol-17 β, for example, has been identified in pregnancy saliva by gas chromatography high resolution mass spectrometry selected ion monitoring of the bis-TMS ether and by gas chromatography mass spectrometry metastable peak monitoring of the bis-tert-butyldimethylsilyl ether. Dehydroepiandrosterone sulphate has been identified in saliva, following enzymic hydrolysis, by gas chromatography high resolution mass spectrometry selected ion monitoring of the tert-butyldimethylsilyl ether and methyl oxime tert-butyldimethylsilyl ether. These initial analyses have been designed to guide the development of routine immunoassay procedures which may subsequently be validated by comparison with reference gas chromatographic mass spectrometric methods." @default.
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- W2031490147 date "1980-11-01" @default.
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- W2031490147 title "Analyses of steroids in saliva using highly selective mass spectrometric techniques" @default.
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- W2031490147 doi "https://doi.org/10.1002/bms.1200071109" @default.
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