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- W2031554008 abstract "Abstract Three simple ruthenium nitrosyl complexes of the compositions [ Et 4 N][RuCl 4 (NO)(DMS O )] ( 1 ), [ Bu 4 N][RuCl 4 (NO)(DMS O )] ( 2 ), and [ Ph 4 P][RuCl 4 (NO)(H 2 O)]·DMSO ( 3 ); where DMSO = dimethyl sulfoxide, Et = ethyl, Bu = butyl and Ph = phenyl, have been synthesized in the single crystal form and their molecular and crystal structures have been determined. The Ru(II) centre is six-coordinated by four chlorido ligands in the equatorial plane and by the N (from NO + ) and O (from DMS O in 1 and 2 , H 2 O in 3 ) atoms in the axial positions forming an RuCl 4 NO donor set. The complexes have been also characterized by infrared and electronic spectroscopies, conductivity measurements, and thermogravimetric (TG) and differential thermal (DTA) analyses. The spectroscopic investigation is consistent with the {Ru(NO)} 6 formulation with NO + coordinated to the diamagnetic Ru(II) centre. The geometries of the complex anions as well as spectroscopic properties were calculated at the B3LYP/LANL2DZ/cc-pVTZ level of theory. These results were compared with those experimentally determined." @default.
- W2031554008 created "2016-06-24" @default.
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- W2031554008 date "2010-08-01" @default.
- W2031554008 modified "2023-09-26" @default.
- W2031554008 title "X-ray structures and spectral characterization of simple ruthenium(II) nitrosyl complexes involving the [RuCl4(NO)(DMSO)]− or [RuCl4(NO)(H2O)]− complex anions" @default.
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- W2031554008 doi "https://doi.org/10.1016/j.molstruc.2010.05.033" @default.
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