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- W2031559553 abstract "Abstract The synthesis of the sodium salt of a new anionic heteroscorpionate trispyrazolylborate ligand as of sodium hydrobis(3-phenyl,5-methylpyrazolyl)(3,5-diethylpyrazolyl)borate (NaTp″) was described. Two cobalt(II) complexes: Tp″Co(NCS)(THF) and Tp″CoTp were synthesized and characterized crystallographically. Trispyrazolylborate ligands (Tp″ and Tp) are coordinated in a κ3 fashion in both complexes. The dependence of the CoN bond length from the steric hindrance of the Tp″ ligand was discussed. The steric hindrance imposed by the Tp″ ligand was also probed by in situ conversions of Tp″Co(NCS)(CD3OD) into Tp″Co(lactate) and Tp″CoTp with 1H NMR spectral monitoring and compared with other similar systems." @default.
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- W2031559553 date "2003-02-01" @default.
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- W2031559553 title "Complexes of heteroscorpionate trispyrazolylborate ligands. Part IX. X-ray crystallographic studies on cobalt(II) complexes of hydrobis(3-phenyl,5-methylpyrazolyl)(3,5-diethylpyrazolyl)borate" @default.
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- W2031559553 doi "https://doi.org/10.1016/s0277-5387(03)00002-0" @default.
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