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- W2031797777 abstract "Rapid kinetics of electron transfer (ET) reactions across the interface between water and 1,2-dichloroethane were measured by steady-state voltammetry at nanopipet electrodes (50- to 400-nm orifice radius). The origins of previously reported imperfect voltammetric responses of ET reactions at micropipets were investigated. Several new experimental systems were explored, and two of them yielded high-quality voltammograms suitable for kinetic experiments. The determined standard rate constants were compared to those measured previously at polarized and nonpolarized liquid/liquid interfaces. The effect of the interfacial dimensions on the magnitude of the apparent ET rate constant is discussed. A new approach to ET kinetic measurements based on the use of the scanning electrochemical microscope with a nanopipet tip and a metallic substrate has been developed and employed to check the validity of determined kinetic parameters." @default.
- W2031797777 created "2016-06-24" @default.
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- W2031797777 date "2005-12-10" @default.
- W2031797777 modified "2023-10-18" @default.
- W2031797777 title "Electron Transfer Kinetics at Polarized Nanoscopic Liquid/Liquid Interfaces" @default.
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- W2031797777 doi "https://doi.org/10.1021/ja055091k" @default.
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