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- W2031873655 abstract "6-O-Acetyl-2,4-diazido-3-O-benzyl-2,4-dideoxy-β-D-glucopyranosyl chloride and 2,6-diazido-3,4-di-O-benzyl-2,6-dideoxy-β-D-glucopyranosyl chloride are two valuable building units suitable for the synthesis of α-linked disaccharides containing 2,4-diamino-2,4-dideoxy- or 2,6-diamino-2,6-dideoxy-D-glucose as nonreducing moieties. The glycoside synthesis is accomplished stereoselectively under mild conditions in the presence of silver perchlorate. The α-(1→3)-linked disaccharides 2,4-diacetamido-2,4-dideoxy-3-O-(2,4-diacetamido-2,4-dideoxy-α-D-glucopyranosyl)-D-glucopyranose and 2-acetamido-2-deoxy-3-O-(2,6-diacetamido-2,6-dideoxy-α-D-glucopyranosyl)-D-glucopyranose have been prepared. Das 6-O-Acetyl-2,4-diazido-3-O-benzyl-2,4-didesoxy-β-D-glucopyranosylchlorid und 2,6-Diazido-3,4-di-O-benzyl-2,6-didesoxy-β-D-glucopyranosylchlorid stellen zwei wertvolle Bausteine zur Herstellung von α-verknüpften Disacchariden mit 2,4-Diamino-2,4-didesoxy- oder 2,6-Diamino-2,6-didesoxy-D-glucose als nicht reduzierende Endgruppe dar. Die Glycosidsynthese gelingt bei Gegenwart von Silberperchlorat stereoselektiv unter milden Bedingungen. Die α-(1→3)-verknüpften Disaccharide 2,4-Diacetamido-2,4-didesoxy-3-O-(2,4-diacetamido-2,4-didesoxy-α-D-glucopyranosyl)-D-glucopyranose und 2-Acetamido-2-desoxy-3-O-(2,6-diacetamido-2,6-didesoxy-α-D-glucopyranosyl)-D-glucopyranose wurden dargestellt." @default.
- W2031873655 created "2016-06-24" @default.
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- W2031873655 date "1979-02-01" @default.
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- W2031873655 title "Stereoselektive synthese von α-verknüpften polyaminodesoxy-zucker-disacchariden mit hilfe der azid-methode" @default.
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- W2031873655 doi "https://doi.org/10.1016/s0008-6215(00)83775-1" @default.
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