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• W2032093325 abstract "Combined wide-angle X-ray diffraction (WAXD) and small-angle X-ray scattering (SAXS) studies using synchrotron radiation were carried out to investigate the structural development during in-situ solution spinning of poly(p-phenylenebenzobisoxazole) (PBO) in poly(phosphoric acid) (PPA). WAXD patterns indicated that the structure in the extruded PBO/PPA dope before coagulation (in water) possessed lyotropic “biaxial nematic” nematic order involving PBO−PPA complex as the mesogenic unit. A different biaxial nematic order in pure PBO was found to develop immediately upon coagulation in water. When the coagulation time exceeded 30 min, the complex PBO/PPA structure completely disappeared, and well-oriented PBO crystals were formed. The meridian peaks exhibited long streaks, indicating a translational disorder of PBO molecules in the fiber direction. SAXS patterns of the PBO fiber after coagulation showed equatorial streaks with no further maxima observed, which is attributed to a microvoid structure." @default.
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• W2032093325 date "2001-12-13" @default.
• W2032093325 modified "2023-10-17" @default.
• W2032093325 title "In-Situ Synchrotron WAXD/SAXS Studies of Structural Development during PBO/PPA Solution Spinning" @default.
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• W2032093325 doi "https://doi.org/10.1021/ma010249g" @default.
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