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- W2032111112 abstract "Solid-state 2H nuclear magnetic resonance line shapes have been obtained from folded films of oriented Li-DNA molecules with the purine bases selectively labeled with deuterium at the 8-position. From line shape simulations, the static base tilts as well as the anisotropic motional amplitudes were determined as a function of hydration level and temperature. It was found that the average tilt angle of the bases is close to 0 ° and at a hydration of ten water molecules per nucleotide the distribution width of tilt angles about this average cannot be larger than 9 ° (standard deviation). A slightly increased distribution width is observed at low hydration levels. The motional amplitudes are hydration dependent, with the tilting motion ranging from 4 ° for the driest, up to 15 ° for the wettest sample, and slightly larger amplitudes are observed for the twisting motion. The amplitude of the twisting motion is unaffected by a temperature decrease down to −60 °C, in contrast to the tilting motion that is suppressed at low temperatures." @default.
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- W2032111112 date "1988-07-01" @default.
- W2032111112 modified "2023-09-27" @default.
- W2032111112 title "Static disorder and librational motions of the purine bases in films of oriented Li-DNA" @default.
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- W2032111112 doi "https://doi.org/10.1016/0022-2836(88)90461-5" @default.
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