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- W2032153110 abstract "2(C6H5)3AsO · H2SeO3 kristallisiert orthorhombisch in der Raumgruppe Fdd2—C2v19 mit a = 20,472(9), b = 32,747(1), c = 10,008(8) Å und Z = 8; d (ber./gef.) = 1,527/1,52 g · cm−3. Die Struktur wurde anhand von 808 unabhängigen Reflexen mittels Patterson- und Fourier-Synthesen bestimmt und nach der Kleinste-Quadrate-Methode bis zu einem R-Wert von 0,056 verfeinert. In der Verbindung sind jeweils zwei (C6H5)3AsO-Einheiten über kurze H-Brücken [O …︁ H …︁ O-Abstand 2,48(4) bzw. 2,35(4) Å] mit einer Selenit-Gruppe verknüpft. Die AsO-Abstände betragen 1,64(9), die SeO-Abstände 1,69(3), 1,83(3) bzw. 1,76(3) Å. Crystal and Molecular Structure of 2(C6H5)3AsO · H2SeO3 2(C6H5)3AsO · H2SeO3 crystallizes in the orthorhombic space group Fdd2—C2v19, with a = 20.472(9), b = 32.747(1) and c = 10.008(8) Å and Z = 8; d (calc./obs.) = 1.527/1.52 g · cm−3. The structure has been determined from 808 independent reflections by Patterson- and Fouriersyntheses, and has been refined by least squares methods to R = 0.056. In the compound two (C6H5)3AsO-units and one selenite group are linked by short H-bonds [O …︁ H …︁ O-distance 2.48(4) resp. 2.35(4) Å]. The AsO-distances are 1.64(9), the SeO-distances are 1.69(3), 1.83(3), resp. 1.76(3) Å." @default.
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- W2032153110 date "1976-07-01" @default.
- W2032153110 modified "2023-09-26" @default.
- W2032153110 title "Kristall- und Molek�lStruktur von 2(C6H5)3AsO � H2SeO3" @default.
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- W2032153110 doi "https://doi.org/10.1002/zaac.19764240211" @default.
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