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• W2032567714 abstract "The bidentate, water-soluble phosphine ligands, bis(bis(hydroxymethyl)phosphino)benzene (HMPB, 1) and bis(bis(hydroxymethyl)phosphino)ethane (HMPE, 2) were reacted with the organometallic precursor fac-[ReBr3(CO)3]2-, 3, to produce the complexes fac-[Re(OH2)(CO)3L]+ and fac-[ReBr(CO)3L] (L = HMPE, HMPB), respectively, in good yields. The rhenium complexes fac-[ReBr(CO)3HMPB], 5, and fac-[ ReBr(CO)3HMPE], 8, were characterized using 1H and 31P NMR spectroscopy. The structure of fac-[ReBr(CO)3HMPB] was confirmed by single-crystal X-ray spectroscopy. The substitution reactions of HMPE/HMPB with the rhenium precursor 3 in aqueous solution were monitored using time-dependent 31P NMR techniques. A significant discrepancy in the reaction kinetics and the substitution mechanism between the two bidentate ligands could be observed presumably due to the different chemical backbones." @default.
• W2032567714 created "2016-06-24" @default.
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• W2032567714 date "2001-04-06" @default.
• W2032567714 modified "2023-09-23" @default.
• W2032567714 title "Development of Novel Water-Soluble, Organometallic Compounds for Potential Use in Nuclear Medicine: Synthesis, Characterization, and ¹H and ³¹P NMR Investigations of the Complexes <i>fac</i>-[ReBr(CO)₃L] (L = Bis(bis(hydroxymethyl)phosphino)ethane, Bis(bis(hydroxymethyl)phosphino)benzene)" @default.
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• W2032567714 doi "https://doi.org/10.1021/ic001284r" @default.
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