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- W2032597399 abstract "Abstract Kim's serendipitous synthesis of a novel cavitand by the one-pot reaction between phloroglucinol and ninhydrin was revisited and extended. A much deeper cavitand was obtained by replacing ninhydrin with benzo[f]ninhydrin. Performing the reaction in a stepwise manner, employing both ninhydrin and benzo[f]ninhydrin, provided ‘mixed bowls’ of lower symmetry. Other cyclic polyketones, such as 1,2-indanedione and alloxan, form with phloroglucinol only partially closed structures. Crystallographic studies of the intermediate compounds in this reaction confirm Kim's postulate that the bowl formation involves hemiketal ring-openings and rearrangements." @default.
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- W2032597399 date "2009-09-01" @default.
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- W2032597399 title "The reaction between phloroglucinol and vic polycarbonyl compounds: extension and mechanistic elucidation of Kim's synthesis for bipolarofacial bowl-shaped compounds" @default.
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- W2032597399 doi "https://doi.org/10.1016/j.tet.2009.07.056" @default.
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