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- W2032654940 abstract "The 1H NMR spectra of HMCo3(CO)12 (M=Fe or Ru) and HFeCo3(CO)12−x[P(OR)3]x (x=1–3, R=CH3; x=3, R=C2H5 or C6H5) showed very broad signals centered near δ=−21 at 27 °C. The band widths were generally smaller for the compounds of larger molecular volume, at lower temperatures and with higher viscosity of the solvent. These data were interpreted in terms of the quadrupole effects of 59Co nuclei to which the hydride proton was μ3-bonded. Supporting evidence was obtained from the 31P and 59Co NMR spectra and the relaxation time T1 of HFeCo3(CO)9[P(OCH3)3]3." @default.
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- W2032654940 title "<sup>59</sup>Co Quadrupole Effects on the<sup>1</sup>H,<sup>31</sup>P, and<sup>59</sup>Co NMR Spectra of HFeCo<sub>3</sub>(CO)<sub>9</sub>[P(OCH<sub>3</sub>)<sub>3</sub>]<sub>3</sub>and the<sup>1</sup>H NMR Spectra of Other Derivatives" @default.
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