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• W2032734515 abstract "A microwave-assisted hydrothermal synthesis route was developed for LT-LiCoO2 and compared with the conventional hydrothermal synthesis. Our X-ray diffraction, magnetisation, and electron microscopy and electrochemical studies in both cases indicate phase-pure and practically stoichiometric materials with Li-content ≥0.99. The microwave-assisted procedure allows reducing the synthesis temperature down to 170 °C which yields plate-like nano-sized LT-LiCoO2 compared to the conventionally synthesized micro-scaled material. These differences clearly show-up in the cyclic voltammetry and the galvanostatic intermittent titration technique data which are used for further characterisation of the materials. In both cases, a tiny non-stoichiometry is suggested by the presence of low-temperature small high-spin Co4+-ions. Our results show that the microwave-assisted process allows lower synthesis temperatures for practically stoichiometric LT-LiCoO2 which is associated to size-reduction of the resulting crystallites down to the nanometre-scale and a higher fraction of the competing spinel phase." @default.
• W2032734515 created "2016-06-24" @default.
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• W2032734515 date "2012-07-01" @default.
• W2032734515 modified "2023-10-14" @default.
• W2032734515 title "Microwave-assisted hydrothermal synthesis of low-temperature LiCoO2" @default.
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• W2032734515 doi "https://doi.org/10.1016/j.solidstatesciences.2012.04.033" @default.
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