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• W2032809924 abstract "An amide-linked ferrocene dimer, [(CH(3)CONHC(5)H(4))Fe(C(5)H(4)CONHC(5)H(4))Fe(C(5)H(4)CONHCH(3))] (7), and a monomer, [(CH(3)CONHC(5)H(4))Fe(C(5)H(4)CONHCH(3))] (5), were synthesized, and their unique structures were determined by X-ray analysis. Amide planes are stacked with respect to each other in both crystal and dilute solution. These complexes form intermolecular NH.O=C hydrogen bonds in the crystal. On the other hand, they form intramolecular NH.O=C hydrogen bonds in a dilute solution as established by IR and (1)H NMR measurements. Spectral data suggest the presence of flapping structures in solution. Crystal data for 5: triclinic, P&onemacr;, a = 9.358(3) Å, b = 9.947(4) Å, c = 7.946(3) Å, alpha = 106.86(3) degrees, beta = 113.15(3) degrees, gamma = 76.59(3) degrees, V = 644.9(5) Å(3), Z = 2. 7.(1)/(2)EtCN: orthorhombic, Pna2(1), a = 7.467(4) Å, b = 14.048(4) Å, c = 23.400(5) Å, Z = 4." @default.
• W2032809924 created "2016-06-24" @default.
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• W2032809924 date "1998-12-01" @default.
• W2032809924 modified "2023-09-26" @default.
• W2032809924 title "An Amide-Linked Ferrocene Dimer, [(CH₃CONHC₅H₄)Fe(C₅H₄CONHC₅H₄)Fe(C₅H₄CONHCH₃)]. Formation of Inter- and Intramolecular NH···OC Hydrogen Bonds" @default.
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• W2032809924 doi "https://doi.org/10.1021/ic9806939" @default.
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