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• W2032990234 abstract "The present paper describes the feasibility of on-line preconcentration of nickel ions from aqueous medium on Ni(II)-imprinted cross-linked poly(methacrylic acid) (IIP) synthesised through a double-imprinting method and their subsequent determination by FAAS. The proposed method consisted in loading the sample (20.0 mL, pH 7.25) through a mini-column packed with 50 mg of the IIP for 2 min. The elution step was performed with 1.0 mol L−1 HNO3 at a flow rate of 7.0 mL min−1. The following parameters were obtained: quantification limit (QL) – 3.74 µg L−1, preconcentration factor (PF) – 36, consumption index (CI) – 0.55 mL, concentration efficiency (CE) – 18 min−1, and sample throughput – 25 h−1. The precision of the procedure assessed in terms of repeatability for ten determinations was 5.6% and 2.5% for respective concentrations of 5.0 and 110.0 µg L−1. Moreover, the analytical curve was obtained in the range of 5.0–180.0 µg L−1 (r = 0.9973), and a 1.64-fold increase in the method sensitivity was observed w..." @default.
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• W2032990234 date "2014-03-05" @default.
• W2032990234 modified "2023-10-02" @default.
• W2032990234 title "Application of Ni(II)-imprinted cross-linked poly(methacrylic acid) synthesised through double-imprinting method for the on-line preconcentration of Ni(II) ions in aqueous media" @default.
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• W2032990234 doi "https://doi.org/10.1080/03067319.2014.891110" @default.
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