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- W2033152224 abstract "Cyclopentadienyllanthanidhalogenide reagieren mit 1,4-Diaryl-butadienen in Gegenwart von Alkalimetallen unter Bildung von Cp*La(1,4-Ph2C4H4) · DME (I), Cp*La(1,4-{o-CH3OC6H4}2C4H4) · 2DME (II), [Li(THF)3][Sm(1,4-Ph2C4H4)2] (III), [Li(DME)][(1,4-{p-CH3C6H4}2C4H4)LuCl2] (IV) und [Li(DME)][(1,4-{o-CH3OC6H4}2C4H4)LuCl2] (V). Samariumtrichlorid reagiert mit 1,4-Diphenylbutadien und Lithium in Tetrahydrofuran zu [Li(THF)4][Sm(1,4-Ph2C4H4)2] (VI), Samarium mit dem p-Tolylderivat in Gegenwart von Iod zu (1,4-{p-CH3C6H4}2C4H4)SmI · 3THF (VII).Die Verbindungen wurden elementaranalytisch sowie durch ihre 1H-, 13C-NMR-, IR- und EI-MS-Spektren charakterisiert.Contributions to Organolanthanide Chemistry. III. Synthesis and Properties of 1,4-Diaryl-1,3-butadiene Lanthanide ComplexesCyclopentadienyllanthanide halides react with 1,4-diarylbutadienes in the presence of alkali metals to give Cp*La(1,4-Ph2C4H4) · DME (I), Cp*La(1,4-{o-CH3OC6H4}2 · C4H4) · 2DME (II), [Li(THF)3][Sm(1,4-Ph2C4H4)2] (III), [Li(DME)][(1,4-{p-CH3C6H4}2C4H4)LuCl2] (IV) and [Li(DME)][(1,4-{o-CH3OC6H4}2C4H4)LuCl2] (V). Samariumtrichloride reacts with 1,4-diphenyl-butadiene and lithium in tetrahydrofurane with formation of [Li(THF)4][Sm(1,4-Ph2C4H4)2] (VI). Reaction of samarium with the p-tolyl derivative in the presence of iodine gives (1,4-{p-CH3C6H4}2C4H4)SmI · 3THF (VII).The compounds were characterized by elementary analysis, i.r., 1H- and 13C- n.m.r., and EI-MS spectra." @default.
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- W2033152224 date "1995-08-01" @default.
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- W2033152224 title "Beitr�ge zur Organolanthanidchemie. III [1]. Darstellung und Eigenschaften von 1,4-Diaryl-1,3-butadien-Komplexen der Lanthanide" @default.
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- W2033152224 doi "https://doi.org/10.1002/zaac.19956210806" @default.
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