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• W2033488049 endingPage "4190" @default.
• W2033488049 startingPage "4183" @default.
• W2033488049 abstract "The reaction of alkyn-1-yl(vinyl)silanes R2Si(CCR1)CHCH2 [R = Me (1), Ph (2); R1 = tBu (a), Ph (b), SiMe3 (c)] with 9-borabicyclo[3.3.1]nonane in a 1:1 ratio affords the 1-silacyclopent-2-ene derivatives 4a–c (R = Me) and 5a–c (R = Ph) as a result of selective intermolecular 1,2-hydroboration of the vinyl group, followed by intramolecular 1,1-organoboration of the alkynyl substituent. The analogous reaction sequence converts the alkyn-1-yl(allyl)dimethylsilanes 3a,c into the 1-silacyclohex-2-ene derivatives 7a,c. All reactions were monitored by 29Si NMR spectroscopy and the structural assignment of the final products was based on multinuclear magnetic resonance data (1H, 11B, 13C and 29Si NMR). The molecular structure of 6a was determined by X-ray analysis." @default.
• W2033488049 created "2016-06-24" @default.
• W2033488049 creator A5061603797 @default.
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• W2033488049 creator A5091875084 @default.
• W2033488049 date "2005-11-01" @default.
• W2033488049 modified "2023-09-23" @default.
• W2033488049 title "An efficient route to substituted 1-silacyclopent-2-enes and 1-silacyclohex-2-enes via consecutive 1,2-hydroboration and 1,1-organoboration" @default.
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• W2033488049 doi "https://doi.org/10.1016/j.ica.2005.03.016" @default.
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