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- W2033532109 abstract "New formate (1–3; 4b, 6 and 7), acetate (8, 9) and trifluoroacetate (12, 13 and 15) complexes have been synthesized and characterized by elemental analysis and by IR and 1H and 13C NMR spectroscopies. New data or new synthetic procedures are provided for several known complexes (4a, 5, 19, 11 and 14). X-ray structural data for cis-Ru(bpy)2(CO)(OCHO)(PO2F2) (4b) clearly identify the η1-bound formate ligand bound to an octahedral ruthenium center and the data for fac-Re(CO)3(PPh3(OCOMe) (9) show an η2-bound acetate ligand bound to an octahedral rhenium center. Infrared spectral data for four types of formate complexes, three bonding types of acetates and the two known types of trifluoroacetate ligands are discussed. Comparisons of the vOCO bands for the carboxylate ligands in all of the complexes show that these bands are useful in identifying the bonding type of each carboxylate ligand." @default.
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- W2033532109 date "1999-03-01" @default.
- W2033532109 modified "2023-10-16" @default.
- W2033532109 title "Synthesis and characterization of ruthenium, rhenium and titanium formate, acetate and trifluoroacetate complexes. Correlation of IR spectral properties and bonding types" @default.
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- W2033532109 doi "https://doi.org/10.1016/s0277-5387(98)00414-8" @default.
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