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- W2033584611 abstract "Abstract The onset of dynamics and the structural changes of octamethyl–ethinyl-ferrocene around a solid–solid phase transition at 248 K have been investigated using the novel technique of quasielastic nuclear forward scattering (QNFS) in a temperature range between 61 and 257 K at a photon energy of 14.413 keV, as well as X-ray powder diffraction at various energies. A pronounced hysteresis for both the dynamical and the structural properties is observed and confirmed by differential-scanning calorimetry. We assign the observed phenomena to a first-order transition from a low-symmetry low-temperature phase to a high-symmetry high-temperature plastically crystalline phase with nearly cubic symmetry. Possible mechanisms for this transition are discussed in the light of our results." @default.
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- W2033584611 date "2003-04-01" @default.
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- W2033584611 title "Structure and dynamics of octamethyl-ethinyl-ferrocene: an organometallic rotator phase" @default.
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- W2033584611 doi "https://doi.org/10.1016/s0022-3697(02)00376-1" @default.
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