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- W2033817060 abstract "Sodium azide reacts with FeH2(dmpe)2 ({Bd1a}) [dmpe = 1,2-bis(dimethylphosphino) ethane] in methanol solution to form FeH(N3)(dmpe)2 ({Bd3a}) and, finally, Fe(N3)2(dmpe)2 ({Bd2}). The bis(azide) complex may also be generated from FeCl2(dmpe)2 ({Bd4a}) by a ligand exchange reaction. The azide ligand is easily replaced by terminal alkynes to form bisacetylide iron complexes. The X-ray crystal structure of Fe(N3)2(dmpe)2 ({Bd2a}) shows that the azide groups are mutually trans and that the NNN groups are essentially linear and tilted by approximately 132° with respect to the plane containing the Fe and four P atoms." @default.
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- W2033817060 date "1995-09-01" @default.
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- W2033817060 title "Synthesis and reactions of azido complexes of iron" @default.
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