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- W2033882055 abstract "The Spherisorb silica/sorbed water system has been investigated at coverages 0.018 ⩽Θ/gH2O g–1SiO2⩽ 0.36 using 1H n.m.r. in the temperature range 190 ⩽T/K ⩽ 300 and also at coverages 0.013 ⩽Θ/gH2O g–1SiO2⩽ 0.033 using dielectric techniques at ambient temperature. In cases where multilayer adsorption occurs there is a discontinuity in the temperature dependence of the n.m.r. linewidth accompanying a freezing phenomenon. Water molecules making up the first loosely packed adsorbed layer (complete at Θ= 0.06 gH2O g–1SiO2) remain mobile at low temperatures at all coverages. Dielectric measurements reveal another discontinuity at a coverage of ca. 0.023 gH2O g–1SiO2. Below that coverage the strength of binding of sorbed water increases with decreasing coverage, while at higher coverages additional water leads to a marked increase in the mobility of the first layer." @default.
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- W2033882055 date "1985-01-01" @default.
- W2033882055 modified "2023-10-18" @default.
- W2033882055 title "Nuclear magnetic resonance and dielectric relaxation investigations of water sorbed by Spherisorb silica" @default.
- W2033882055 doi "https://doi.org/10.1039/f19858100847" @default.
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