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- W2033889110 abstract "The Heck-Matsuda (HM) reactions 2 employ arenediazonium salts as arylating agents and present several advantages when compared to traditional protocols (aryl halides or triflates): they are phosphine-free, do not require inert atmosphere, are more economical, and can be carried out at lower temperatures and shorter reaction times. In this work, the HM arylation is evaluated as the key step for the synthesis of combrestatin analogues. RESULTS AND DISCUSSION Dimethyl fumarate was used as substrate for the HM arylation using Pd(OAc)2 as catalyst in MeOH as solvent with a variety of diazonium salts. The reaction performed best in the absence of a base. Higher yields and selectivity were observed for diazonium salts bearing electron-donating groups (Scheme 1)." @default.
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- W2033889110 date "2013-09-01" @default.
- W2033889110 modified "2023-10-03" @default.
- W2033889110 title "Synthetic Studies Towards Combrestatin Analogues via Heck- Matsuda Reaction" @default.
- W2033889110 doi "https://doi.org/10.5151/chempro-14bmos-r0043-1" @default.
- W2033889110 hasPublicationYear "2013" @default.
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