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- W2034122189 abstract "A 2D layer complex 1 and a linear trinuclear complex 2 with mixed ligands have been synthesized and characterized by elemental analyses, IR and single-crystal X-ray diffraction. In 1, the Mn(II) ions are six-coordinated and lie in distorted octahedron coordination environments. Complex 1 is connected into a 2D layer structure based on a linear trinuclear Mn3(admtrz)4(N3)6 (admtrz = 4-amino-3,5-dimethyl-1,2,4-triazole) building unit with either (6,3) topology when Mn1 cations as three-connected nodes or (4,4) network when the coordination trinuclear units being regarded as four connected nodes. In 2, the Co(II) ions are in slightly distorted octahedron coordination geometries. The magnetic behaviors are investigated in the temperature range 1.8–300 K. The magnetic susceptibility measurements show that the Mn(II) ions of complex 1 are weakly antiferromagnetically coupled with g = 1.98(1), J1 = −6.31(5) cm−1 and J2 = −1.88(1) cm−1. There is dominant zero field splitting (ZFS) effects with g values, g// = 2.38(2) and g⊥ = 4.96(4), indicated a significant presence of the spin–orbit coupling and magnetization experiment reveals large, uniaxial zero-field splitting parameters of D = −29.55 cm−1 for 2." @default.
- W2034122189 created "2016-06-24" @default.
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- W2034122189 date "2011-05-01" @default.
- W2034122189 modified "2023-10-16" @default.
- W2034122189 title "Trinuclear-based coordination compounds of Mn(II) and Co(II) with 4-amino-3,5-dimethyl-1,2,4-triazole and azide and thiocyanate anions: Synthesis, structure and magnetic properties" @default.
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- W2034122189 doi "https://doi.org/10.1016/j.ica.2011.01.029" @default.
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