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- W2034132667 abstract "Diethylzinc reacts with hydroperchlorates of N-alkylated 1,3,5-triazacyclohexanes (R3TAC; R = methyl (Me), benzyl (Bz), isopropyl (iPr)) and with the hydrotetrafluoroborate of 1,3,5-tris-(para-fluorobenzyl)-1,3,5-triazacyclohexane (FBz3TAC) to give the corresponding cationic zinc ethyl complexes [(R3TAC)Zn(Et)][X] (X = ClO4−, BF4−). Similar complexes were obtained from diethylzinc treated with [HNMe2Ph][BF4] or [HNMe2Ph][B(C6F5)4](Et2O) in the presence of R3TAC (R = Bz, FBz, s-1-phenylethyl (s-PhMeCH)). A product of decomposition of [(Bz3TAC)Zn(Et)][ClO4] was analyzed by X-ray diffraction. The structures of [({s-PhMeCH}3TAC)Zn(Et)][BF4] an [(FBz3TAC)Zn(Et)][BF4] were estimated using nuclear Overhauser enhancement spectroscopy. Protonolysis of diethylzinc with [HNMe2Ph][BF4] in the presence of 13-benzyl-1,5,9-triazatricyclo[7.3.1.05,13]-tridecane (BzTATC) yielded the complex [(BzTATC)Zn(Et)][BF4]." @default.
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- W2034132667 date "1996-08-01" @default.
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- W2034132667 title "The chemistry of 1,3,5-triazacyclohexane complexes 5: cationic zinc(II) alkyl complexes of N-alkylated 1,3,5-triazacyclohexanes and 13-benzyl-1,5,9-triazatricyclo[7.3.1.05,13]-tridecane" @default.
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- W2034132667 doi "https://doi.org/10.1016/0022-328x(96)06271-7" @default.
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