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• W2034141743 endingPage "5102" @default.
• W2034141743 startingPage "5097" @default.
• W2034141743 abstract "Sulforaphene (4-methylsulfinyl-3-butenyl isothiocyanate), which has significant chemopreventive activities, is an important phytochemical ingredient produced by myrosinase hydrolysis of glucoraphenin (4-methylsulfinyl-3-butenyl glucosinolate) found in radish seeds. In this research, we found that sulforaphene was unstable and converted rapidly to a water-soluble degradation product in the hydrolytic process. The degradation product was successfully purified by preparative high-performance liquid chromatography on a C18 column using 10% methanol in water as the mobile phase. On the basis of MS and NMR spectroscopy data, the degradation product was identified to be 6-[(methylsulfinyl)methyl]-1,3-thiazinan-2-thione. The degradation pathway of sulforaphene was proposed in our study. Furthermore, low pH and metal ions were also found to have an effective inhibition to the degradation reaction of sulforaphene. Through adjusting the pH value of the system or adding metal ions after the content of sulforaphene has reached its maximum, the yield of sulforaphene increased significantly compared with that of the control." @default.
• W2034141743 created "2016-06-24" @default.
• W2034141743 creator A5002868353 @default.
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• W2034141743 creator A5056532273 @default.
• W2034141743 creator A5061694243 @default.
• W2034141743 creator A5072360502 @default.
• W2034141743 date "2013-05-20" @default.
• W2034141743 modified "2023-09-28" @default.
• W2034141743 title "Instability and Structural Change of 4-Methylsulfinyl-3-butenyl Isothiocyanate in the Hydrolytic Process" @default.
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• W2034141743 doi "https://doi.org/10.1021/jf400355d" @default.
• W2034141743 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/23688308" @default.
• W2034141743 hasPublicationYear "2013" @default.
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