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- W2034143486 abstract "Crystallization of synthetic trans-1,4-polyisoprene (TPI) at −20°C in hexane and amylacetate solutions gave chain-folded α-type crystals with 53% and 57% crystallinity, respectively. Selective ozonolysis degradation of the isoprene units in the surface folds associated with high-resolution g.p.c. measurement was used to determine the crystalline stem length, stem length distribution and fold surface structure of the α-TPI crystals. As ozone uptake increased, the isoprene units of the main fraction of oligomer products were found to decrease from 13, reaching a constant value at 11 for hexane and 12 for amylacetate. The polydispersity of the oligomer fractions was found to be in the range of 1.01–1.02. These findings suggested that the chain fold structure might be tight folding with slightly irregular folds, with a stem length of 11 monomers and a dispersion of 2.3 for lamellae grown from hexane, and 12 monomers with dispersion of 2.3 for those grown from amylacetate." @default.
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- W2034143486 date "1993-01-01" @default.
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- W2034143486 title "Structure of solution-grown trans-1,4-polyisoprene crystals: 1. Determination of stem length and fold surface structure by ozonolysis-g.p.c. measurement" @default.
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- W2034143486 doi "https://doi.org/10.1016/0032-3861(93)90590-7" @default.
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